Taguchi- Grey relational analysis for Optimizing the Compressive Strength and Porosity of Metakaolin-Based Geopolymer

Document Type : Original Article

Authors

Department of Ceramics Engineering and Building Materials, Faculty of Materials Engineering, University of Babylon, Babylon, Iraq

Abstract

Geopolymer is of the promising eco-friendly materials that can be produced with variety of physical and mechanical properties through alerting the processing parameters. Obtaining Geopolymer with high compressive strength and high porosity may make this material as a preferred candidate for many thermal and physiochemical applications. This research aims to identify the set of the processing parameters that yield such as these Geopolymer materials. Taguchi method combined with Grey relational analysis has been used to solve this multi response trouble. The analysis and the experimental results showed that it is possible to achieve this aim by using low amount of hydrogen peroxide as foaming agent, low amount of yeast as catalyst, and low amount of vegetable oil as a stabilizer. Furthermore, the polymerization time elapse before adding the foaming agent is found to be important processing parameter. Also, the experimental results showed that high porosity and adequate compressive strength can be obtained at the same geopolymer body by choosing the suitable values of the processing parameters. Moreover, it has been found that the use of yeast as catalyst and the polymerization time are important processing parameters. Also, it has been noticed that the amount of the vegetable oil, which is used as stabilizer, should be kept in low values to obtain the optimal compressive strength and porosity

Keywords


  1. A. Alves, A. Nogueira, E. Vazquez, and S. de Barros, “A bibliographic historical analysis on geopolymer as a substitute for portland cement,” Key Engineering Materials, Vol. 834, (2020), 127-131, doi.org/10.4028/www.scientific.net/KEM.834.127
  2. Petlitckaia and A. Poulesquen, “Design of lightweight metakaolin based geopolymer foamed with hydrogen peroxide,” Ceramics International, Vol. 45, No. 1, (2019), 1322-1330, doi.org/10.1016/j.ceramint.2018.10.021
  3. Ducman and L. Korat, “Characterization of geopolymer fly-ash based foams obtained with the addition of Al powder or H2O2 as foaming agents,” Materials Characterization, Vol. 113, (2016), 207-213, doi.org/10.1016/j.matchar.2016.01.019
  4. B. E. Boum et al., “Thermal behaviour of metakaolin-bauxite blends geopolymer: microstructure and mechanical properties,” SN Applied Sciences, Vol. 2, No. 8, (2020), 1-12, doi.org/10.1007/s42452-020-3138-9
  5. Bobirică, C., Orbeci, C., Bobirică, L., Palade, P., Deleanu, C., Pantilimon, C.M., Pîrvu, C. and Radu, I.C.,, “Influence of red mud and waste glass on the microstructure, strength, and leaching behavior of bottom ash-based geopolymer composites,” Scientific Reports, Vol. 10, No. 1, (2020), 1-12, org/10.1038/s41598-020-76818-4
  6. N. Assi, K. Carter, E. Deaver, and P. Ziehl, “Review of availability of source materials for geopolymer/sustainable concrete,” Journal of Cleaner Production, Vol. 263, (2020), 121477, doi.org/10.1016/j.jclepro.2020.121477
  7. Yan, Y. Guo, Z. Ma, Z. Zhao, and F. Cheng, “Quantitative analysis of crystalline and amorphous phases in pulverized coal fly ash based on the Rietveld method,” Journal of Non-Crystalline Solids, Vol. 483, No. 1, (2018), 37-42, doi.org/10.1016/j.jnoncrysol.2017.12.043
  8. M. Novais, G. Ascensão, L. H. Buruberri, L. Senff, and J. A. Labrincha, “Influence of blowing agent on the fresh- and hardened-state properties of lightweight geopolymers,” Materials & Design, Vol. 108, (2016), 551-559, doi.org/10.1016/j.matdes.2016.07.039
  9. N. Khattak, M. A. M. Khraisheh, and S. Gul, “Porosity control of self-supported geopolymeric membrane through hydrogen peroxide and starch additives Porosity control of self-supported geopolymeric membrane through hydrogen peroxide and starch additives,” Desalination and Water Treatment, Vol. 152, (2019), 10-15, DOI: 10.5004/dwt.2019.23895
  10. Lertcumfu, K. Kaewapai, P. Jaita, R. Sanjoom, G. Rujijanagul, and T. Tunkasiri, “Synergistic effect of animal oil or butter and hydrogen peroxide on physical and mechanical properties of porous alumino-siliceous materials,” ScienceAsia, Vol. 46 S, No. 1, (2020), 58-65, doi:10.2306/scienceasia1513-1874.2020.S008
  11. B. Singh, “Fly ash-based geopolymer binder: A future construction material,” Minerals, Vol. 8, No. 7, (2018), doi.org/10.3390/min8070299
  12. Rizal, A. P. Pratama, Khamistan, A. Fauzi, Syarwan, and A. Azka, “Effect of H2O2 as the Foaming Agent on the Geopolymer Mortar using Curing of Room Temperature,” IOP Conference Series: Materials Science and Engineering, Vol. 854, No. 1, (2020), DOI: 10.1088/1757-899X/854/1/012022
  13. A. Jaya, L. Yun-Ming, H. Cheng-Yong, M. M. A. B. Abdullah, and K. Hussin, “Correlation between pore structure, compressive strength and thermal conductivity of porous metakaolin geopolymer,” Construction and Building Materials, Vol. 247, (2020), p. 118641, doi.org/10.1016/j.conbuildmat.2020.118641
  14. Qin Shuai, Zhonghui Xu, Zhengzhen Yao, Xiaoyue Chen, Zao Jiang, Xi Peng, Ran An, Yu Li, Xin Jiang and Han Li “Fire resistance of phosphoric acid-based Geopolymer foams fabricated from Metakaolin and hydrogen peroxide,” Materials Letters, 263, (2020), 1-4, doi.org/10.1016/j.matlet.2019.127228
  15. Anggarini, S. Pratapa, V. Purnomo, and N. C. Sukmana, “A comparative study of the utilization of synthetic foaming agent and aluminum powder as pore-forming agents in lightweight geopolymer synthesis,” Journal of Open Chemistry, Vol. 17, No. 1, (2019), 629-638, DOI:10.1515/chem-2019-0073
  16. Yan, F. Zhang, X. Feng, J. Kong, B. Wang, and J. Yang, “Effect of high temperature on the mechanical properties of hierarchical porous cenosphere/geopolymer composite foams,” Journal of Applied Ceramic Technology, Vol. 18, No. 3, (2021), 817-829, doi.org/10.1111/ijac.13681
  17. Kränzlein, H. Pöllmann, and W. Krcmar, “Metal powders as foaming agents in fly ash based geopolymer synthesis and their impact on the structure depending on the Na /Al ratio,” Cement and Concrete Composites, Vol. 90, (2018), 161-168,
  18. Hajimohammadi, T. Ngo, P. Mendis, T. Nguyen, A. Kashani, and J. S. J. van Deventer, “Pore characteristics in one-part mix geopolymers foamed by H2O2: The impact of mix design,” Materials & Design, Vol. 130, No. 15, (2017), 381-391, doi.org/10.1016/j.matdes.2017.05.084
  19. Pantongsuk, T., Kittisayarm, P., Muenglue, N., Benjawan, S., Thavorniti, P., Tippayasam, C., Nilpairach, S., Heness, G. and Chaysuwan, D., “Effect of hydrogen peroxide and bagasse ash additions on thermal conductivity and thermal resistance of geopolymer foams,” Materials Today Communication, Vol. 26, (2021), 102149, doi.org/10.1016/j.mtcomm.2021.102149
  20. Cui, D. Wang, J. Zhao, D. Li, S. Ng, and Y. Rui, “Effect of calcium stearate based foam stabilizer on pore characteristics and thermal conductivity of geopolymer foam material,” Journal of Building Engineering, Vol. 20, (2018), 21-29, doi.org/10.1016/j.jobe.2018.06.002
  21. Bai, T. Ni, Q. Wang, H. Li, and P. Colombo, “Porosity, mechanical and insulating properties of geopolymer foams using vegetable oil as the stabilizing agent,” Journal of the European Ceramic Society, Vol. 38, No. 2, (2018), 799-805, doi.org/10.1016/j.jeurceramsoc.2017.09.021
  22. Bai and P. Colombo, “High-porosity geopolymer membrane supports by peroxide route with the addition of egg white as surfactant,” Ceramics International, Vol. 43, No. 2, (2017), 2267-2273, doi.org/10.1016/j.ceramint.2016.10.205
  23. Lertcumfu, K. Kaewapai, P. Jaita, T. Tunkasiri, S. Sirisoonthorn, and G. Rujijanagul, “Effects of olive oil on physical and mechanical properties of ceramic waste-based geopolymer foam,” Journal of Reinforced Plastics and Composites, Vol. 39, No. 3-4, (2020), 111-118, doi.org/10.1177/0731684419896852
  24. Qiao, Y., Li, X., Bai, C., Li, H., Yan, J., Wang, Y., Wang, X., Zhang, X., Zheng, T. and Colombo, P., “Effects of surfactants/stabilizing agents on the microstructure and properties of porous geopolymers by direct foaming,” Journal of Asian Ceramic Societies, 9, No. 1, (2021), 412-423, doi.org/10.1080/21870764.2021.1873482
  25. D. Van Rest and D. J. Cowden, “Statistical Methods in Quality Control.,” Applied Statistics., Vol. 7, No. 3, (1958), p. 202, doi.org/10.1177/0008068319570306
  26. A. A. Al-Dujaili, I. A. D. Al-Hydary, and Z. Z. Hassan, “Optimizing the Properties of Metakaolin-based (Na, K)-Geopolymer Using Taguchi Design Method,” International Journal of Engineering, Transactions A: Basics, Vol. 33, No. 4, (2020), 631-638, Doi:10.5829/IJE.2020.33.04A.14
  27. Arıcı, E. Çelik, and O. Keleştemur, “An analysis of the engineering properties of mortars containing corn cob ash and polypropylene fiber using the Taguchi and Taguchi-based Grey Relational Analysis methods,” Case Studies in Construction Materials, Vol. 15, (2021), e00652. doi.org/10.1016/j.cscm.2021.e00652
  28. K. Prusty and B. Pradhan, “Multi-response optimization using Taguchi-Grey relational analysis for composition of fly ash-ground granulated blast furnace slag based geopolymer concrete,” Construction and Building Materials, Vol. 241, (2020), p. 118049, doi.org/10.1016/j.conbuildmat.2020.118049.
  29. M. Hsu, A. Cheng, S. J. Chao, J. R. Chang, L. W. Teng, and S. C. Chen, “The grey relational analysis of quality investigation of concrete containing solar PV cells,” 4thInternational Conference on Engineering and Innovative Materials (ICEIM 2015), Section: Materials Science and Engineering, Vol. 27, No. MATEC Web of Conferences, Article No. 01006, 1-4, (2015). doi.org/10.1051/matecconf/20152701006
  30. Keleştemur and E. Arıcı, “Analysis of some engineering properties of mortars containing steel scale using Taguchi based grey method,” Journal of Building Engineering, Vol. 29, p. 101015, 2020. https://doi.org/10.1016/j.jobe.2019.101015
  31. C. Yaragal, B. C. Kumar, and K. Mate, “Optimization of ferrochrome slag as coarse aggregate in concretes,” Computers and Concrete, Vol. 23, No. 6, (2019), 421-431, DOI: http://dx.doi.org/10.12989/cac.2019.23.6.421
  32. Zhang, W. Qiao, Y. Wu, Z. Fan, and L. Zhang, “Multi-Response Optimization of Ultrafine Cement-Based Slurry Using the Taguchi-Grey Relational Analysis Method,” Materials, MDPI, Vol. 14, No. 1, (2021), 1-23, doi.org/10.3390/ma14010117
  33. T. Çöğürcü and M. Uzun, “The Taguchi optimization of mechanical and durability properties of accelerator added concrete,” Journal of Polytechnic, Vol. 0900, 0-2, 2021. DOI: 10.2339/politeknik.857525
  34. Z. H. M. A. Ahmed Al-dujaili, I. A. Disher Al-hydary, “Experimental Improvment of Geopolymer-Cement Properties Using Taguchi Method,” University of Babylon, 2019.
  35. R. Marakia , H. Tagimalek, M. Azargomanb, H. Khatamic , M. Mahmoodib . Experimental Investigation and Statistical Modeling of the Effective Parameters in Charpy Impact Test on AZ31 Magnesium Alloy with V-shape Groove Using Taguchi Method, International Journal of Engineering, Transactions C: Aspetcs, Vol. 33, No. 12, (2020), 2521-2529, DOI: 10.5829/ije.2020.33.12c.13
  36. Khezrloo, M. Tayebi, A. Shafiee, and A. Aghaie, “Evaluation of compressive and split tensile strength of slag based aluminosilicate geopolymer reinforced by waste polymeric materials using Taguchi method,” Materials Research Express, Vol. 8, No. 2, (2021), DIO: 10.1088/2053-1591/abe101/meta
  37. I. Qazi, M. Abas, R. Khan, W. Saleem, C. I. Pruncu, and M. Omair, “Experimental investigation and multi-response optimization of machinability of AA5005H34 using composite desirability coupled with PCA,” Metals (Basel), Vol. 11, No. 2, (2021), 1-24, doi.org/10.3390/met11020235
  38. B. Saedon, N. Jaafar, and M. Azman, “Multi-objective optimization of titanium alloy through orthogonal array and grey relational analysis in WEDM,” Procedia Technology, Vol. 15, (2014), 832-840, DOI: 10.1016/j.protcy.2014.09.057
  39. Rajput, S. S. Pundir, M. Goud, and N. M. Suri, “Multi-Response Optimization of ECDM Parameters for Silica (Quartz) Using Grey Relational Analysis,” Silicon, Vol. 13, No. 5, (2021), 1619-1640, doi.org/10.1007/s12633-020-00538-7
  40. Sayed, R. A. Gado, S. M. Naga, P. Colombo, and H. Elsayed, “Influence of the thermal treatment on the characteristics of porous geopolymers as potential biomaterials,” Materials Science and Engineering: C, Vol. 116, (2020), 111171. doi.org/10.1016/j.msec.2020.111171
  41. Cheng-Yong, L. Yun-Ming, M. M. A. B. Abdullah, and K. Hussin, “Thermal Resistance Variations of Fly Ash Geopolymers: Foaming Responses,” Scientific Report, Vol. 7, (2017), 1-11, DOI: 10.1038/srep45355